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DOI: 10.1016/j.bbagen.2012.09.008

The collected samples were resuspended in a 0.1% formic acid solution (0.1% formic acid, 2% acetonitrile, and 98% Milli-Q water) and analyzed on an Eksigent C18 column (150 mm 75 m, 3 m) using a gradient mobile phase of 98% acetonitrile, 2% Milli-Q water (A) and 0.1% formic acid (B) at a flow rate of 0.3 L/min